ازمایش 3 Making alcohol-derived data

. Alcohol, the most common derivative derivative. making spirits 3 and 5-Nitro phenyl benzoate, ethyl acetate and aortanha. You may also use the alpha-نفتیل polyurethane but the test used for more fnlaha. In all cases after the product was pure solid Crystal melting point earns using the reference tables, the type of alcohol. Preparation of 3 and 5 di Nitro benzoate: combine 3 and 5 Dec نیتروبنزوئیل chloride with alcohols, Ester comes and get the corresponding procedures for the first, second and third type of alcohols. Especially for الکلهایی that dissolve in water and may have a very slight amount of water can be helpful

1) liquid alcohols:

in a test tube is completely dry 2 30 30 hot with alcohol about half 3و5 di Nitro بنزوییل chloride mixture, and continue to simmer gently for 5 minutes. About 10 30 30 ml distilled water and add it to the solution in an ice bath to cool the product into the hands of China. Collect the raw product and with 10 30 30 2% sodium carbonate and water-solution using the atanolmajdda field. Solvent for recrystallization to finalise the work must be a minimum size to be

۲)of solid alchol :

solid alcohol at 5 30 30 and a half grams of dry-diaminopyridine solve Nitro بنزوییل DVD 3و5 chloride to add it. Mix bahalt رفلاکس heat for 15 minutes. The reaction mixture is cold and in a solution of sodium carbonate includes 5 cool CC 5 CC of water and 5%. Soluble in cold ice bath to keep up the sediment. By smooth bokhner fuel, and wash with water. Then with ethanol solvent – water noblor (recrystallization) again Preparation of the test method: پارانیتروبنزوات and benzoate: a) 1 cc of alcohol at 3 CC dry and it solved diaminopyridine tepid benzoyl chloride or پارانیتروبنزوئیل dichloride. After the termination of the initial reaction, the mixture slowly to the blaze on the heat for 1 minute, and then to the sorts of things while program at 10 CC of water. After the Lees of sediments, pour it out the top of the liquid. Remaining with 5 CC of 5% sodium carbonate scrubbing and data by filter paper with ethanol and recrystallization The method of preparation of a derivative of the alpha نفتیل polyurethane (polyurethane α-نفتیل): a gram of alcohol or phenol without water in a test tube and 5.0 ml ISO phenyl cyanate to add it. If the unknown compound, phenol should be reacting with 2 or 3 drops of diaminopyridine or ethanolamine waterless کاتالیز. If the reaction to the case itself has failed, the solution for 5 minutes on a hot steam bath. Then the desired solution in a cold ice content of human and the human wall, glass scratch together woman, through the کریستالیزه crystallization and accelerating. Polyurethane prepared by dissolving it in a 5 ml petroleum ether or carbon Tetra chloride recrystallization. Urethane derivative: (2cc) 1gr ISO cyanate 5grفنیل alcohol mixture inside Ben Mari did, the resulting Crystal cold and drying after doubling its melting point Physical properties: create a crystal water sediment factors: the presence of error within the reaction that causes the break down of the derivative carbon dioxide and gas been free urethane. The safety of phenyl cyanate ISO: identify the potential effects of acute health risks:: in the case of inhalation is very dangerous. In case of skin contact (irritant), of eye contact (irritant), consumption is dangerous. In case of contact with skin, a little dangerous. Exposure to it too severe, it can toandmanjer to myrrh

The effects of chronic alcoholic:

athrsartan potential: not available. Mutagenic effects: mutagenic to bacteria and/or yeast. First aid measures: eye contact:. Check for and remove any contact lenses in case of contact, immediately eyes with plenty of water for at least 15می. Skin contact:. In case of contact, immediately flush skin with plenty of water. Breathe:. In case of inhalation, remove to fresh air. Storage: storage: container in a cool, well ventilated area and keep been.. Physical and chemical properties. Mode and the physical appearance: liquid odour: acrid molecular weight: 119.13 grams/Mole color: colorless to light yellow. Clear clear.

Boiling point:

158 ° C (316.4 ° F) C-168. Melting point:-30 ° C (-22 ° Its melting point شتقی. that is sure to have to dry. the derivative caot contain solvent and dry season has not yet detailed the melting point. May find the derivative of درآزمایشگاه may not be possible for all common combinations we can have an article if we mix it with the derivative melting point it finds the correct diagnosis we pay reduction but did not find the melting point decrease if it is properly diagnosed. We are based on a systematic method of chemical groups all we this classification the classification based on the solubility of if we do it wrong leads to error in all stages of the testing should look to the amount of کمیتهای material non-compliance can lead to errors if you use too much ازrege Nt leads to error in performing the test. Urethane derivative in making sure to be solved in phenylisocyanate بایدالکل if it is not unknown for the melting point article halshden is not free and the melting point is for phenyl isocyanate The

derivative test erroore :

melting point it gets dry it would have taken. the derivative caot contain solvent and dry season has not yet detailed the melting point. May find the derivative of درآزمایشگاه may not be possible for all common combinations we can have an article if we mix it with the derivative melting point it finds the correct diagnosis we pay reduction but did not find the melting point decrease if it is properly diagnosed. We are based on a systematic method of chemical groups all we this classification the classification based on the solubility of if we do it wrong leads to error in all stages of the testing should look to the amount of کمیتهای material non-compliance can lead to errors if you use too much ازrege Nt leads to error in performing the test. Urethane derivative in making sure to be solved in phenylisocyanate بایدالکل if it is not unknown for the melting point article halshden is not free and the melting point is for phenyl isocyanate .initrobenzoic acid From Wikipedia, the free encyclopedia Jump to: navigation, search 3,5-Dinitrobenzoic acid is an organic chemical that is an important corrosion inhibitor and is also used in photography. This aromatic compound is used by chemists to identify alcohol components in esters and in the fluorometric analysis of creatinine. References[edit] Jump up ^ CRC Handbook of Tables for Organic Compound Identification, Third Edition, 1984, ISBN 0-8493-0303-6. Literature[edit] "3,5-dinitrobenzoic acid". Combined Chemical Dictionary. Chapman and Hall/CRC Press. 2007. B. C. Saunders, G. J. Stacey, I. G. E. Wilding: "The Preparation of 3:5-Dinitrobenzoic Acid and 3:5-Dinitrobenzoyl Chloride – Observations on the Acylation of Amino-acids by means of 3:5-Dinitrobenzoyl Chloride and certain other Acid Chlorides", Biochem. J., 1942, 36 (3–4) p. 368–375; Text https://en.wikipedia.org/wiki/3,5-Dinitrobenzoic_acid Phenylisocyanate Phenylisocyanate is an organic compound typically abbreviated PhNCO. The molecule consists of a phenyl ring attached to the isocyanate functional group. It is a colourless liquid that reacts with water. Phenylisocyanate has a strong odor and tearing vapours, therefore it should be handled in the fumehood. Characteristic of other isocyanates, it reacts with amines to give ureas.[1] Similarly, reacts with alcohols to form carbamates. It is used in addition with triethylamine to activate nitro groups to undergo (C,O) 1,3-dipolar cycloaddition (as opposed to O,O). The nitro group (RCH2NO2) is converted to RCNO in the reaction, with CO2 as one of the by products.[2] References[edit] Jump up ^ Emmanuil I. Troyansky "Phenyl Isocyanate" in Encyclopedia of Reagents for Organic Synthesis, 2001 John Wiley & Sons doi:10.1002/047084289X.rp073 Jump up ^ Mukaiyama, Teruaki; Hoshino, Toshio (1960). "The Reactions of Primary Nitroparaffins with Isocyanates". Journal of the American Chemical Society 82: 5339. doi:10.1021/ja01505a017 https://en.wikipedia.org/wiki/Phenylisocyanate